I wonder where the failure is. Recovered under 300mg of crude tar from 360g of finely powdered MHRB.
MHRB was based with NaOH and extracted with toluene.
Resulting extract was freeze percipated and the toluene decanted.
Toluene residue was air dried and then dissolved in acetone.
The resulting asetone solution was then mixed with cannabis leaf.
Bioassay of said mixture was rewarding. Definitely active product.
But the yield was questionably low.
Multiple extractions to the same material will be pursued.
This whole process of going thru 1.5kg of bark has prowided low yeilds.
The Cake method was used for the first 200g with utter failure, it does not work with finely powdered bark.
But een going thru the first kg of raw material, only about 1.5g of pure white solid was produced.
MHRB was based with NaOH and extracted with toluene.
Resulting extract was freeze percipated and the toluene decanted.
Toluene residue was air dried and then dissolved in acetone.
The resulting asetone solution was then mixed with cannabis leaf.
Bioassay of said mixture was rewarding. Definitely active product.
But the yield was questionably low.
Multiple extractions to the same material will be pursued.
This whole process of going thru 1.5kg of bark has prowided low yeilds.
The Cake method was used for the first 200g with utter failure, it does not work with finely powdered bark.
But een going thru the first kg of raw material, only about 1.5g of pure white solid was produced.


