Mescaline Sulfate

DrugPhreak · Working Bee

Damn! SWIDP can't wait to try some mescaline!!! Shocked

Instead of distilling the toluene from the freebase evaporating it in a beaker should work fine since mescaline freebase has such a high boiling point at atmospheric pressure right? Or would it form the carbonate by doing so and need an A/B again or would some other issue come into play here, which I'm not aware of? Wouldn’t just evaporating the toluene from amphetamine freebase work ok too? I don’t see why it wouldn’t.

IndoleAmine · Dreamreader Deluxe

transistor child · gnome

M.Hcl has very low solubility in IPA, probable same for the sulfate.
But why not just dissolve the freebase in toluene (dried with magnesium sulfate first) and gas it with hydrochloric acid?

IndoleAmine · Dreamreader Deluxe

Because it doesn't make the sulfate.. Laughing

(seriously: gassing needs pure freebase, cacti extractions are seldomly really pure unless several a/b's are part of the procedure)

The sulfate is rather soluble in IPA (contrary to what was expected), and has to be crashed out by adding acetone or ether until a lasting turbidity can be seen, followed by prolonged cooling in the freezer to crystallize all sulfate.

But the advantage is that you can make a pure salt even from rather dirty/impure M.freebase.

Just don't use too much IPA in the beginning, as stated.

transistor child · gnome

Ah, sorry. Didn't know we talked about extracted mescaline (maybe I should have read the complete thread).

loki · guinea pig

the why not of gassing - cos it takes fancy gear to do gassing and less than fancy gear risks the evil white vapours turning everything steel in sight into a brown crusting wreck. given fancy gear, gassing is loovlee

transistor child · gnome

Nah.
Creating HCL-gas is easy, and all the gear it requires is a bottle and a rubber hose that can withstand the acid (and something to gas oufcourse). With good ventilation, no problems (and if you don't have good ventilation you shouldn't do any reactions at all). It's the eeeeasy part of any synthesis.