rxtalization of 2-(chloroacetamido)-5-chlorobenzop

[starlight]

Hi there,

anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be?

many thanks.

[java]

Maybe by checking out this article , you can find your answer.......java

One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone

CHINESE JOURNAL OF PHARMACEUTICALS, 26, 49,1995


it may be archived here.....

http://zgyygy.periodicals.net.cn/default.html

I found the reference here using a korean search engine.....

http://science.empas.com/search/kisti_detail.html?sn=20051743033

[Rhodium]

Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7]

119-121°C   (ethanol) J.Org.Chem. 27, 562 (1962)
117-118°C   (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962)
117-118°C   (benzene, diethyl ether, petroleum ether)

Patent DE1136709

(Chem.Abstr. 59, 12827, 1963)