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DMSO autoxidation

Started by pablos, June 30, 2004, 04:38:00 AM

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pablos

Have anyone already tried the autoxidation of anethole with dmso?
The procedure papers give exellent yeld (77%) of ketone in only 8
hours at 120 grad.
I have 25 grams pure anethole at home and 100 ml dmso but I can´t find  the ratio in this papers  and I speak not japans.Any good idea?

Rhodium

We are not mind-readers. Use the post linking feature.


pablos

Sorry I tought it was a well known document.

https://www.thevespiary.org/rhodium/Rhodium/pdf/isosafrole.dmso.oxidation.pdf


this is the paper in japan