Cold temps kept it the dark color
50c- got lighter/white
60c- light yellow/orange, some dark oil droplets being thrown around
65c- darker yellow/orange, same or similar amount of oil, no more produced(possibly)
70c- darker orange
75c darker orange, temp shutoff
The ferret appeared to have a decent amount of this dark orange oil and thought success! NO, fail. Upon extraction, extraction is black. A/B lead to a very very small white/yellow oil, which pretty much gave nothing. Whered it all go?!?!?
1. One idea is to keep the temp under 60c or so. Once the oil droplets formed, it appears that no more oil was being created as the temp rose higher to 65-70-75c. The mix just appeared to get overall darker in color. Just an idea, shut off at 60c.
2. Aqueous layer was dripped on hot base, and extraction led to nearly nothing
3. Oil layer extraction, upon cooling had brownish particulate settle to bottom, this is supposedly unreacted amide and was filtered off.
All visual cues lead to success, somewhere along extraction, a/b perhaps something went wrong. What if that black oil extraction was dried, and directly gassed instead? Ferret knows, scary looking shit extraction, but direct gassing would bring black crystals idk hahahaha!
Ferret doesnt know if anyone will respond, but there is her note. When will this hoffman be someones bitch!