Author Topic: Most efficient method for cannabis extraction,need help...  (Read 375 times)

lugh

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Re: Most efficient method for cannabis extraction,need help...
« Reply #20 on: February 17, 2011, 10:45:43 PM »
Quote
I don't see why coffee percolator can't be used!

Petroleum ether vapor is flammable  ::)  A percolator made from a glass bottle with a hole drilled in the bottom works quite well for small scale extraction  8)
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Oerlikon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #21 on: February 18, 2011, 12:56:21 AM »
No shit! :D

When you only have buds simple reflux is enough,
percolator will be used for trimmings.
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jon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #22 on: February 18, 2011, 03:36:52 AM »
soxhlet extraction is better because the pot gets exposed to fresh solvent, percolator would work just as well.

letters

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Re: Most efficient method for cannabis extraction,need help...
« Reply #23 on: February 18, 2011, 10:27:25 PM »
did you try out the methods suggested? or just write here back and forth? seems like you have been given all the answers...
like before, alkanes are best, quick isopropanol wash comes a close second.
there is really no need for reflux, and like jon said, soxhlet is much better. Ive found that 2-3 room temp extractions with alkanes works satisfactory, gives good yields, and is very easy to do. Ive done it up with up to 600g of low grade arabian cannabis. got roughly 40-50g of honey colored oil, which vaporizes fully with no residue.
i suggest you try out one of the methods instead of discussing it to oblivion.

Oerlikon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #24 on: February 18, 2011, 11:08:43 PM »
Actually I menaged to buy a bit of oil before I got chance to extract from plant material
but there is nothing bad in discussing how to do it right once I have it!
People answered trying to help,so I tought it was rude not to answer on topic I started.

Plant is drying right now and I will report back when I try one of the methods.
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letters

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Re: Most efficient method for cannabis extraction,need help...
« Reply #25 on: February 21, 2011, 01:54:44 AM »
good luck!

lugh

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Re: Most efficient method for cannabis extraction,need help...
« Reply #26 on: February 21, 2011, 02:31:45 AM »
The Hive post on constructing a percolator from sheet metal:

https://the-collective.ws/forum/index.php?topic=19973

People have caused their houses to burn down trying to extract cannabis with acetone  :o  Flammable vapors are very dangerous  8)
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Oerlikon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #27 on: February 21, 2011, 03:32:28 AM »
I tried to extract with petrolether but had too little.
Used coffe grinder to grind down plant material (25cm long bud) into dust and submerged it into warm
chloroform for 20min sinc I had it handy. Than filtered.

Ended up with a deep green solution that is evaporating right now.

Due the lack of attention some of the chloroform was spilled itno
coffe grinder causing some plastic to be solvated and it ended up in extract :(

Will try to evaporate it completely and make glycerine tincture.(For sublingual use)
Hope that plastic will perticipate and go away if I do that.

Rest of the plant material was sawed and it will be extracted with petrolether
once I got it.
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lugh

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Re: Most efficient method for cannabis extraction,need help...
« Reply #28 on: February 21, 2011, 03:38:57 AM »
Hydrocarbons are best due to the fact that they don't extract as many types of compounds  ;)  Polymers will crystallize from cannabis oil if cold enough  8)
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Oerlikon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #29 on: February 21, 2011, 03:44:36 AM »
Yeah...
Low b.p. hydrocarbons are way to go but didn't have them enough at hand...

Thanks on polymers tip!
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TaurineMonster

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Re: Most efficient method for cannabis extraction,need help...
« Reply #30 on: February 21, 2011, 07:16:09 AM »
dude! be careful with thc extracts! I know someone that allmost burned down a million dollar cabin(freakin hippie lol) when they where extracting with butane. they had a glass full of boiling butane being heldby someone, when they went to light a incense charcoal, the flame jumped  from the charcoal to the jar, setting the whole thing on fire. the person spilled some on his hand and burned the FUCK out of himself. He wanted to go to the hospital sooo bad, but what do you say? I burned my self making hashoil. yeah right. think again hippy! next time be more careful and heres some aloe!

happy Xtracting!

also, someone once told me, that if you use buds instead of leaf to make oil, the quality goes WAY up! I believe that is how they make the famous "brown sugar" hash oil.

and if you are dead set on making an extract with a solvent, I heard anhydrous Ethanol is the preferred way. But there are lots of ways to extract cannabis

I prefer full melt bubble hash personally
« Last Edit: February 21, 2011, 07:19:43 AM by TaurineMonster »

overunity33

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Re: Most efficient method for cannabis extraction,need help...
« Reply #31 on: February 21, 2011, 08:00:46 AM »
dude! be careful with thc extracts! I know someone that allmost burned down a million dollar cabin(freakin hippie lol) when they where extracting with butane. they had a glass full of boiling butane being heldby someone, when they went to light a incense charcoal, the flame jumped  from the charcoal to the jar, setting the whole thing on fire. the person spilled some on his hand and burned the FUCK out of himself. He wanted to go to the hospital sooo bad, but what do you say? I burned my self making hashoil. yeah right. think again hippy! next time be more careful and heres some aloe!

happy Xtracting!

also, someone once told me, that if you use buds instead of leaf to make oil, the quality goes WAY up! I believe that is how they make the famous "brown sugar" hash oil.

and if you are dead set on making an extract with a solvent, I heard anhydrous Ethanol is the preferred way. But there are lots of ways to extract cannabis

I prefer full melt bubble hash personally

i think most people here and even most people in general understand the dangers of a cabin full of butane... not to mention you wont find many chemists lighting up incense when working with solvents... even so welcome here and this is quite an interesting thread

especially interested in freezing out hashoil impurities

Oerlikon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #32 on: February 21, 2011, 01:48:47 PM »
ROFLMAO You made my day! That sound like scene from movie "dumb&dumber" or "Just visiting"!  ;D ;D ;D
This is EXACTLY why you shuld not make drugs and use drugs at the same time!

Why the f..k would anyone in his right mind burn incense in (makeshift) lab full of flamable and explosive chemicals!?
Here,people use burning inscence only when dead man is in the house before burial. Those craps only stinks up the whole room!

Back on subject...
I got dark green-yellow tarry solid that becomes fluid when heated and made me high when I
tried to squeez last bit of solvent out of filter. I call that potent!
Leftower plant material also has some potency and will be used for cooking or further extracting
with propper equipment and solvents.

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where you can choose your own dreams!

lugh

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Re: Most efficient method for cannabis extraction,need help...
« Reply #33 on: February 21, 2011, 03:01:06 PM »
Quote
Thanks on polymers tip!

Crystallization is rather challenging, it can take a very long period of time  ;) If a seed crystal is provided it becomes much easier  8)
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The Lone Stranger

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Re: Most efficient method for cannabis extraction,need help...
« Reply #34 on: April 04, 2011, 10:22:54 PM »
I`ve extracted grass and hash with petro-ether , ethyl-alcohol and ethyl-ether and ate the product.The last was the best but probably because there was still ether in it........

I think it`s better to just get the strongest vodka one can get,put the powdered product in a bottle and cover it with vodka.After a few weeks standing in a cool dark place the strained vodka works wonders and i think the quality of the high is better than doing the other extractions.Probably because one looses some with them and the vodka gets it into ones system faster.

Oil is to sticky and goes off to quick too.

hypnos

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Re: Most efficient method for cannabis extraction,need help...
« Reply #35 on: April 04, 2011, 11:58:54 PM »
Oerlikon,, if you filter your extract with paper coffee filters when its in the solution, most of the plant matter and other small particles of  ???  will be removed

 and then upon evaporating (or whatever method you use to remove the solvent) you will be left with a reddish to honey colored oil/resin

  96% Etoh works really well,, and takes less than 24 hours---why make it hard for your self?

  Of course 'buds' are more than likely to have more resin in them than the other parts of the plant....
          
    But as Taurine monster says,,IF you DO have nice resin coated buds,,"Bubble hash" is a great way to make hash,,AS GOOD as most imported hash of high quality--go to you tube and check out Bubble hash,,  which uses ice water and sieves (which you will need to buy,,but they work wonders,,,)

   The first time I saw some 'Bubble hash',,which was, before I had even heard of "bubble hash",,if it hadnt been via someone I knew well and trusted,, I dont think I would have believed it WASNT  Afghani or Nepalese!!!  but it was made with good ole 'seedy heads' in middle Oz :o
  
 It's quite 'unique' IMO

  As for "brown sugar" hash oil?  Thats a new one for me!!! Never even heard of it ???  Maybe 'brown sugar' heroin.....which most certainly made quite a name for itself 'back in the day'...T

  The Strolling Bones,, er the Rolling Stones wrote a song about it IIRC--nor really my type of band except for 4-5 songs of which Gimme Shelter+Paint it Black are two :P  
« Last Edit: April 05, 2011, 12:03:59 AM by hypnos »
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jon

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Re: Most efficient method for cannabis extraction,need help...
« Reply #36 on: April 05, 2011, 01:49:02 AM »
ok this is what i used to do
and it worked very well
hexane/butane is'nt all that polar so you will get incomplete extractions unless you soxhlet it 24 hours or so, so i would just boil it in ethanol strain it through a wire mesh collander.
then evaporate this on table salt the salt would be inert and impart more surface area.
then, i wold chill some butane in the freeze and pour it along with the salt/pot extract into a coke bottle with teflon around the threads.
then, i would slosh it around a bit cool it and then slosh it around again then i would slant the bottle to decant off the butane from the salt and while ice cold i'd crack it open and pour it onto pyrex it would instantly boil off.
this was a very efficient technique.