12-10-03 18:39
(Rated as: UTFSE!)
12-10-03 19:15
(Rated as: UTFSE!)
(Newbee)
12-10-03 20:12
No 475979
Let the acetone evaporate and proceed as usual. With a reaction that size, it should only take a few hours.
Jizzy Jizzy Bang Bang
(Stranger)
12-11-03 09:58
No 476091
Evap off the tone then do the wash...but!
All this was cooked on 99.5C for 3 hours and everything was going perfect.
Where is it written that a rxn under LongWetReflux conditions is going to be complete @ 3hours?
That calculation defy's scientific logic.
Takes a lickin and keeps on tickin