losthope
08-04-04 22:55
      crystal oil
(Rated as: incomprehensible)
    
 
 
 
    evilscripter69
(Hive Bee)
08-05-04 00:49
No 523778
      Gas in the pan?     

Is  methane not a gas??  Did you mean Meth ?
 be more specific, what methods did you use, so on. Maybe then you might get help.
 
 
 
 
    Methodicalman
(Stranger)
08-05-04 02:07
No 523791
      crystal oil     

take your oil,check ph,take one cup warm water,one spoon red devil lye,mix,and pour 1/2 the cup thru your oil,let settle and room temp,check ph again.you want 12 to 14 ph level;before gassing,which will be cut in 1/2 for product when u gas.,,,Before ph-ing...run an aquarium pump (airiate)your oil for a couple hours to get rid of gas.  Use salt and sulphuric, instead of A&M or A&H...better gas better control.On an R$B.,,the PH must be right to GAS  ,unlike shaker way...Humidity will kill any gas return also. 70 degrees with no more than 60% humidity., is ideal.[purple]
 
 
 
 
    geezmeister
(Of Counsel)
08-05-04 07:35
No 523811
      meth oil in a pan?     

You should stir the meth oil in a suitable nonpolar solvent before gassing.

mostly harmless
 
 
 
 
    dextro
(Newbee)
08-05-04 10:25
No 523834
      How much NP is the right ratio to dissolve the     

How much NP is the right ratio to dissolve the FB before gassing ( ex. 20ml FB in ????ml Toluene) ?

After steam distilling of the FB, is then a (5%) NaOH wash recommendable (before H20 and brine) or is this overkill/nonsense?

only water/brine washes are enough?

thx