all_all2009
02-09-04 06:51
      How to Synthesis piperidine?
(Rated as: UTFSE!)
    
 
 
 
    Vitus_Verdegast
(Hive Addict)
02-09-04 07:36
No 487482
      my good man,     

by the reduction of pyridine of course. It's lots of fun as both have a very unagreeable lingering smell.
Was it Milton that said hell smelled sulfurous like? I disagree, I'm sure in hell they have to bathe in pyridine.smile

So now, use the fucking search engine, search at rhodium's page, and you will find what you look for.

http://tinyurl.com/223dg
http://tinyurl.com/2z9gn
 
 
 
 
    Antoncho
(Official Hive Translator)
02-09-04 07:42
No 487484
      UTFSE!     

Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse)
 
 
 
 
    Xicori
(Hive Bee)
02-09-04 10:54
No 487501
      The pyridine reduction in Post 288137 is ...     

The pyridine reduction in Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse) is surely working out nice, but the condensation of 1,5-Dibrompentane´s grignard reagent with the Benzoylpiperidine doesnt work as it should frown

SWIM tried this reaction with very pure reagents 2 times, but never had luck :( Better use your piperidine within another synthetic pathway..