(Stranger)
07-28-04 12:49
No 522273
in benzyl chloride synth on rhodiums site how concentrated doesthe HCl have to be?
(Chief Bee)
07-28-04 14:03
No 522281
Provide a link and tell us exactly which preparation you are referring to - there are several benzyl chloride syntheses on my page.
The Hive - Clandestine Chemists Without Borders
(Stranger)
07-28-04 17:51
No 522340
i am talking about https://www.rhodium.ws/chemistry/benzylc
its the synth that says "Chlorination of benzyl alcohol with conc. HCl "
(Chief Bee)
07-28-04 17:58
No 522341
The stronger acid you use, the higher your yields will be. Concentrated 36-37% HCl is the best to use, but you might get away with using the 31% strength too, just compensate by using a larger excess of acid.
The Hive - Clandestine Chemists Without Borders