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 Subject: pfed hcl 

 

 

 

 

 

 

ayejay
(Hive Bee)
09-21-02 18:03
No 358933

  

  

pfed hcl

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Hello swarm. I stopped by swik's crib and she said the last 3 attempts at reduction via rp/i using the hcl were failures. Now swik earned her wings a couple years ago and told me that soaking in zylene for a day and turps for a dayand then acetone still resulted in failure. Is anybee using hcl and having success or is the freebase the only method that works today? Pfed obtained via numerous trips to the local chain stores. Thanx IJ


Indiana Jones

 

 

 

 

 

 

wareami
(Hive Addict)
09-21-02 20:56
No 358979

  

  

Formulation of Choice....

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will determine the final result based on the extraction method and solvents used. The only radical changes in OTC pfed extraction over the past year seem to have come about as a result of the Formulators including the extended release drymatrix inactives and one other stumbling block to be discussed further down. These drymatrix OTC's can be identified by the 4 inerts that are prefabricated separately then combined into a preferred tablet-pressing technique known as "Dry Compaction" or "Dry Compression".
These 4 inert ingredients are:
•Hydroxypropyl Methylcellulose
•Microcrystalline Cellulose
•Dibasic Calcium Phosphate
•Magnesium Stearate
There are now other patents available that will need to be investigated further to determine how the next formulations will affect bees.
The keys to successful consistancy will vary greatly, but most will always revolve around personal preference based on discovering what works best for you.
When the "Bee Blockers" first surfaced a few years back, they mainly consisted of methocell, the decogestant sidekicks(chlorpheniramine maleate and triprolidine), analgesics, and the big headscratcher Povidone. Pretty much in that order.
Since then, volumes have been written on their successful removal combining chems & technique.
Now the one other stumbling block mentioned above revolves around the cooperation of the Pharm industry and Legal Legislation enforcement.
The inactive listings on many of the OTC products now carry the inclusion of "May also Contain"!
This explicitly presents a whole new playing field in regards to the scorecard..."Success vs Failure".
Now while it might have been assumed that wareami was also placed on that list of Inactives, his 'stestmonkeys have not.
When all the "BeeBlockers" first burst on the scene, Worlock suggested that bees need to find a user friendly brand and stick with it while keeping tabs on lot#'s and dates. That advise is just as valid today as it was then.
When push comes to shove and all the scores are tallied, pound for pound, in terms of yield, the povidone formulations seem the easiest to deal with if they can bee found without the above drymatrix ingredients present in the mix!
Ibeeware informed bees that tetrachloroethylene successfully defeated povidone a few months back when it was put under the knife using the Egull method alone.
Most of the actafool generic brands containing Triprolidine hcl 2.5mg and Pfed hcl 60mg tested successfully.
For the sake of consistancy...the 's stuck with procedure as originally outlined in the Egull method and have yet to have a failure.
Hopefully within a day or two, the 's will deliver a more concise write-UP to ware!
Hope this helps some...
Peaceof the re
action
Have FUN-Bee SAFE





Everything Ibee says should be taken with a Large Grain of Sympathomimetic Amine Salt
ô¿ôWareami

 

 

 

 

 

 

zibarium
(Naked)
09-21-02 22:09
No 359013

  

  

beyond "either/or"?

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labels with "may also contain" lists of gakk might bee worth a mini-extraction, to see if they also contain what they may also contain, or not.

if not, fair bet that identical packs in the same zone could also contain "the short list" of additives.

in swiz's brief experience, the "may also contain" pills did not also contain that which they may have also contained.

i wonder if any bee has found that such packages marked that way, in fact , DO contain the full list of additives that they may also contain?

also, swiz made a comment some time ago, that he thought a 3rd category of pill labels had occurred...that of the outright lie. because he dreamed of a disgusting gooey mess with labels which had previously been honest as to their lack of this stringy goo.

and he wondered if they were 'allowed' to use the trick of not mentioning(at all ) certain harmless additives on the label? certainly a potent tool for the w.o.d., if it is true. lure a bee into a large dream, approached in a fashion that is doomed to fail...based on a printed list of additives.
failures of that sort also tend to bring out the boiling solvents and other histrionics that tend to bring on the law. A lot more stink is generated when ya have to do things over and over.

 

 

 

 

 

 

wareami
(Hive Addict)
09-22-02 08:50
No 359136

  

  

The "Naked Truth"

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Ya got yer birthdaysuitz on? Good! For some strange reason, according to the masters and the Godz, this facilitates successcrazy...
Don't ask me...IT WORKS!laugh
Zib: I hear ya bro...
Beez may have noticed some of the naming conventions that have changed or more precisely, been altered wareas inactives are concerned. These alterations may be subtle enough to satisfy the "Consumer Right to Know" policies, but they reek havoc on determining what exactly is present.
One little undersight can make the difference between using "this solvent" or "that solvent" or incorporating this step or that step!
The aim from the WOD's point of view is to make this a guessing game and at least give them a fifty/fifty chance that beez won't succeed 50% of the time until a remedy is stumbled upon and in this way they have bought enough time to throw another monkey in the barrel!
Techniques like VE's universal, Geez's Waterless A/B, Dwarfers PP/SS, and Ibee's Egull are good failsafes against many of the inactives across the board. Only once in the last year has Ibee been stumped by Gello and that was only when he deliberately ommitted a tetra wash to see what would happen in order to identify with what other bees were reporting and for discovering the best way to proceed if the unfortunate happened!
Geez graciously provided the solution when Ibee presented him with the problem. The key for climbing out the "QuickSand Gello Bowl" isn't grabbing the nearest schtick and beating yourself to death over the dead horse sitting before ya! The horse ain't dead...HE'S TIRED...RUBBERIZED!!! It needs to set til completely dry
before the next assalt!
The other problems that have rear-ended bees dreams are PEG and Polysorbate (tween80).
Ibee has recently read ware some bees are clueing themselves in on the different properties and solubilty issues concerning the different weights of the Polymers being used and the various temps that affect their removal!
Legully, the opposition only needs to include the ingredient listing, they don't need to reveal the individual chemical make-up of the composition.
Jacked and Ibee had a good discussion going at the zonez regarding the various weights and naming conventions being used on Polysorbate, the Oxides, and the FD&C dyes!
All these come into play and are commonly overlooked as being stumbling blocks! The main things to stay updated on are how these chems interact with each other. This requires research, chemistry books as reference, and staying glued to the board. If it's a hunt and peck game til finding a user friendlybrand, then sobeeit!
Those that have their hand in the bottomless cookie jar tend to share with others!
It's all here!
Peaceof the re
action
Have FUN-Bee SAFE



Everything Ibee says should be taken with a Large Grain of Sympathomimetic Amine Salt
ô¿ôWareami

 

 

 

 

 

 

ayejay
(Hive Bee)
09-22-02 10:41
No 359147

  

  

samo samo

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Thanks for all the great info. Swik swears that the feedstock is the same generic redhots that she has used for over a year and that the inactives listed hasn't changed. Everything points to PEG but the 12 hour soaks in xylene does not work as suggested. Yes tetra and turps were employed also. The question remains is freebase the only way to fly here in the heartland? Thanx bees.


Indiana Jones

 

 

 

 

 

 

ChemoSabe
(Hive Addict)
09-23-02 02:11
No 359434

  

  

Relative Success

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Swims buddy is in the process of chucking his old habits and jumping on the VE (of recent "universal extraction" fame) bandwagon.

But just as a test he soaked a few old tyvek wrapped "GUP onions" that still had some leftover residual pfed in them in some dry ISO. The pillstocks for the GUP onions were a combo of generic pearly 120's and de-redded red hots.

The suspected new presence or newly higher concentrations of PEG in these pill formu8lations had begun to get swim's buddy a high ratio of iodometh in what had become his his "shittier than usual" yeilds.

Swim's buddy took the leftover pfed yeild from the GUP onions and gave it a good boil in xylene followed by a good boil in acetone.

End product after rxn had no trace of iodometh in it and the yeild was decent. Leading swims buddy to beleive that if one still wants to pursue tyvek exteactions followed by xylene and acetone boils that a good, clean end product may still bee had. At least for this week that is.

PS. When Steely Dan once sang "PEG, she will come back to you" they weren't kiddin'!


My innate talent for falling flat on my face had once again saved the day.

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-23-02 10:56
No 359531

  

  

jumping on the VE's "universal extraction

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Just a note'' swihft so far has used the VE''universal extraction twice 'and he must say that it works well enough to use''' and the cheap pills you get for a dollar was used just to try  .

However he is still getting shit to carry over even when a mineral spirits presoak and boil followed by tone wash was used first..

The phed was pretty crystals but so is the shit that seeems to follow it thru every cleaning so far.....

yeilds by the way are down'' down'' down.......40 grams total pill mass  11 boxes of 24's  ''''''''only 2 grams freebase clean enough to use....

Swihft thinks ve's method is the way to go 'he just thinks this fake crystal shit that follows needs something to kick it's ass and he's not sure what that would bee..

has to bee others with the same experience '''' let swihft know if the shit happens to you as well......


  "why stop now"  

 

 

 

 

 

 

ChemoSabe
(Hive Addict)
09-23-02 11:21
No 359535

  

  

UniEx Bandwagon Jump

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Hey handsfull2,

The 1st time Swim's buddy tried VE's UniEx technique he got 1 gram of FB crystals out of a 4x20x120 (4 boxes of 20 120's). This gram of FB was then salted into roughly 1 gram of psuedoHCl by addling warm DH20 and 30% muriatic acid to it in a sep funnel, shaking it and vapping the water.

I think it was Geezmeister who warned that doing this without some sort of other cleanup might carry along some additives. So Swim's buddy went ahead and reacted the gram as a test and the end product did show some sign of carry a small bit of iodometh with it in some portions of it's dried crytal pattern. There is nothing esle in swim's buddy setup that could now cause this smidge of Iodo to appear except for the presence of some PEG which swim's buddy assumes was carried over from the psuedo HCl converted from the FB crystals.

Next text of the UniEx has the ground pill mass having been soaked overfnight in Xylene followed by a tone boil.

But swim's buddy would really like to learn to do a "controlled FB rxn" as opposed to his usual "variation on Worlock's PsuedoHCl rxn" but currently the FB rxn territories are uncharted waters for him.


My innate talent for falling flat on my face had once again saved the day.

 

 

 

 

 

 

ayejay
(Hive Bee)
09-23-02 13:22
No 359558

  

  

yeilds

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Swik says 20 boxs 96 count each yeilded 23 grams of the prettiest sudo seen in awhile. Pills were thrashed! Killer reaction 2.5 hrs with all the good signs. Had to base it really hard and for all that work ended up with some kinda syrupy crap that wouldnt dry and barely got ya off. WTF?


Indiana Jones

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-23-02 13:57
No 359572

  

  

yeilds

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yep that's what swihft saw was the crystals in all their Glory ''''he thought wow these are so pure '''' then he did a test and dayummmmmm not pure at all...

but could sure fool someone who had little knowlege of what to look for......

Im sure swihft can do better on yeilds but he does'nt see much better at the moment so any help on this would bee of course greatful......

cool


  "why stop now"  

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-23-02 14:04
No 359576

  

  

UniEx Bandwagon Jump

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Swihft did a fb reaction and everything went well except with a little crap carried over but damn good buzz he tells me..


swihft Never had much luck with those 120's but who knows he's getting closer and closer to making that kill shit again and he can't wait '''' he tells me he misses it....
wink


  "why stop now"  

 

 

 

 

 

 

wareami
(Hive Addict)
09-23-02 18:39
No 359716

  

  

I know I'm not being ignored here!

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Ibee has indicated what that kicker might be!
Try a tetra wash....
It leaves mst crap behind and is not a threat to activating the dry matrix!
However...because of the other sides that have come across when using the 120's Ibee has used other brands that contain POV since Tetra kills the POV!
There is far less shit in the NON-timereleased!
Just give it a shot!
Ibee isn't saying not to go the VE way....He's just suggesting that the kicker needed may be in the tetra!
It takes ten minutes top to do a tetra wash! Then proceed on with the pillmass as usual!
Keep us posted!
Peaceof the RE
action
Have FUN-Bee SAFE


Everything Ibee says should be taken with a Large Grain of Sympathomimetic Amine Salt
ô¿ôWareami

 

 

 

 

 

 

ChemoSabe
(Hive Addict)
09-23-02 19:49
No 359747

  

  

Ignoring the Friendly Little Pill?

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Well, at the risk of being told to UTFSE I'll axe if a certain brand of heavy Dty Brake parts Cleaner that rhymes with Westbone that comes in a spray can will work.

Swim's buddy happens to have a fresh can of it but it remains untested.


My innate talent for falling flat on my face had once again saved the day.

 

 

 

 

 

 

ayejay
(Hive Bee)
09-23-02 19:50
No 359748

  

  

yo u not ignored big guy

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Heavyware, de-redded generics! Tetrawash employed! (by the way, thanx for that one!) Back to the ole drawing board. I remember swik having problems and the turps came charging to the rescue. About a year later tetra to the rescue! You know who you are and many many thanx from the heartland. ij


Indiana Jones

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-23-02 20:05
No 359757

  

  

I know I'm not being ignored here!

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swihft ain't ignoring ibee and the boyz ''''shit took swihft  a full year just to start understanding ibee don't want to let that time go to waste.....

on the tetra '''' swihft has used it before but did'nt use the right stuff '' send him a pm on the ingredents if ibee finds the time......wink

Now watch ibee ignore ole' swihft''''''cool


  "why stop now"  

 

 

 

 

 

 

geezmeister
(Bee of the Month)
09-23-02 22:04
No 359814

  

  

on the freebase pseudo and gakks

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I tested the VE method before it was posted, tried some its early variations. I did the proceedure as written, by the book. The post went up August 17. I had been working with it or close variants of it for better than a month when it was posted. I used it after it was posted until the end of August. At that time I began experimenting with a specific variant of the technique which is too dissimilar to allow any conclusions about the written technique. I have not followed the technique as written for three weeks or more but when I last used it the crystals were very clean, the product from them superb and potent. 

There are contaminants in the naptha which were highly water soluble and will dissolve into any available moisture. Gassing without drying the gas is a good way to extract PEG from that naptha. SWIG has found PEG in every batch of pseudo exracted with water and HCl from the naptha used to extract the pseudo.  It is there. Understand and be aware of it. 

The variant SWIG has been testing gave great yields at the start. It was fast and high yield. It seems very effective with white sixties. The 120's are tougher. In the last three weeks SWIG has noticed that each successive extraction contained more PEG that the last. Think about that.

Saturday's extraction and reaction yielded product laced with PEG-- and as bad as he has ever seen it. These freebase crystals were not extracted by the Straight to Bee method. While he was cleaning the mess up post reaction and recovering as much of the yield as he could, SWIG kept noting that PEG did not have the same solubilities it did the last time he had the problem.

The PEG in this mess is in fact the viscuous brown oily fluid it should be. It is unaffected by freezing. It can ge rinsed from meth with dry acetone-- and that did not work before. It dissolves readily in ISOheet. That's right. (And SWIG tried four bottles from different vendors and dried one bottle dried over epsoms salts. Same results every time. SWIG could grow meth crystals even with the PEG in the mix, unlike before. Over and over, he noted that the PEG in the batch was not the same PEG.

SWIG has a hunch that the molecular weight of the PEG in the time relase 120's being manufactured today is a different weight PEG that was being put in the 120's in May and June of this year. The PEG has been "tuned" to be soluble not only in water but in dry alcohols, and in some non-polar solvents. The reason the problem seems to be getting worse is that the stocks of pills with the old PEG are now pretty well depleted and replaced with fresh stock laden with the newer PEG. SWIG recalls a bee's comment that a xylene soak did not remove the PEG. This would be consistent with SWIG's hunch about the solubilities being tampered with. He also noted in the cleanup that the PEG in this batch behaved differently at higher temps, and could be extracted from non-polar solvent if the solvent were boiled and some ground carbon added. Again, this did not work the last time SWIG saw the problem.

The problem may be the PEG getting a tuneup. And our techniques needing to improve to meet that fact.

Others might keep an eye out for other solubility differences.

If you have freebase crystals and suspect PEG is in the batch, you should rinse them well with dH20. Unless the PEg is in the freebase crystal, water should dissolve it.

If you want to lower the chance of PEG further, do a couple of xylene boils of the GUPs before processing them.


Mostly harmless

 

 

 

 

 

 

zibarium
(Naked)
09-23-02 23:59
No 359855

  

  

geez, are you sherlock holmes?

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i love this cat and mouse aspect of the w.o.d.!

it brings out the smarts in a chemhacker, or any other hacker.

geez, someday they'll make an additive in your honor...after foiling the activated carbon.

if i was to second guess the guessers, i'd try to get in their corner, and design something that would fuck up yours, or v.e.'s latest side-stepping.  what would it bee? how clever can they get with these additives, and keep it all edible?

what would you come up with, to fuck with yourself in this extraction effort, if you were a highly paid legit chemist, working on new gakk formulations?

apologies for the drift, mate.

and later on:

cleaning red-hots via/high speed machine blasts; followed by high decibel heavy metal sound waves.

swiz has seen the false and lovely crystals.
he suspects these to bee the source of flask-neck crystals. they look hard, but are more like jello.

 

 

 

 

 

 

wareami
(Hive Addict)
09-24-02 05:46
No 359932

  

  

The Pep Boyz!

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Ibee and the Kidz have noticed that thare favorite brand of Egull juice has been yanked from the shelf completely in his local....Does that mean that they no longer make it? Who Nose!!! It unlikely that the industry will completely stop making that formulation of Cleaner as it is Environment Friendly! The brand was the made by the same manufacturers of Worlocks highly publicized Diethyl source years back!
In it's place were two different formulations made by another company.
One Good to GO and the other wasn't.
Tetrachloroethylene and Carbon Dioxide were the only listed ingredients in the good to GO one!
Ibee suspects that every major Autoparts Supplier will have what is needed.
SWIHFT and Chemo:
Ibee said he will PM you guyz later! He's got some Grinding to do!
Geez: Ibee and the Kidz have yet to employ the latest. Mainly because of real-estate space and they want to do it buy the book as suggested! But will soon! They also have never run FB but it looks FUN! So that isn't FAR off either!

Peaceof the RE
action
Have FUN-Bee SAFE



Everything Ibee says should be taken with a Large Grain of Sympathomimetic Amine Salt
ô¿ôWareami

 

 

 

 

 

 

ayejay
(Hive Bee)
09-24-02 15:10
No 360079

  

  

yanked from shelves

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Heavyware, All that is a purchasing decision to go with a cheaper vender. Hey, that place has a very slim margin and purchasing a cheaper product might mean a bigger bonus at bonus time. It's getting very hard to maintain a steady high around here in the heartland. As a matter of fact, steady is out the window and occasional is sketchy @ best.
   Swik did dissolve some of that gooey mess in some meoh and filter. Swik let sit for about 1 week (Forgot about that crap), and upon re=discovery! Green shards 1 " long.
2 tone washes cleared up the shards and Swik was so excited to get off she ingested a tad too much and had to pop a couple valiums lest she pop a vein in the ole thinker. ij


Indiana Jones

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-26-02 21:32
No 361107

  

  

got it

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about VE'S UNIVERSAL SWIHFT did the ole third time's a charm thing I guess '' he changed a couple things that got him a nice return and clean at that.

No tetra wash  or pre soak this time ''' but next time he thinks he might give it a try
the only thing different was he left the pill stock sit over night in the base ' he did'nt add any dh20 or tone 'just let it sit over night.

what a difference in return and wow the product is real pretty long glass half inch darlins and all about the same size '
he went in with 3 boxes of 48 60's ' got back almost 4 grams and thats like 3 times better then what he got back before..

He has used the universal three times the first two he had very little success with return so he thinks the over nite base is what did it for him   ... 
  cool


  "I'm not really here "  

 

 

 

 

 

 

ChemoSabe
(Hive Addict)
09-26-02 23:21
No 361143

  

  

Overnight Basing

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Thanks handsful (looks like "glandsful" from your icon there) for your valuable experimenting explorership.

Swim's buddy has a batch ground up & about to begin it's journey thru the UniEx process again and he'll definitely try the ovenight basing trick.

Have you yet tried an FB rxn? That's nexts on swim's buddy's agenda. Rumors of a more potent end product have him very curious about it.


I've fallen into a bottomless pit and I can't get it up.

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-27-02 04:21
No 361179

  

  

Have you yet tried an FB rxn?

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Yes'' it seems to have a better kick IMHO. '''''''     


  "I'm not really here "  

 

 

 

 

 

 

Jacked
(Ancient Alchemist Delux)
09-27-02 07:46
No 361218

  

  

Try this

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Plenty of acetone, I mean high volume, 10:1.   Then hot naptha untill no more clouds, decant the fine silt on off, dont let it settle, Thats all it takes. The reaction will take care of the rest. (based on 96 count red dots)


The end result is directly connected to the effort applied

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-27-02 08:25
No 361227

  

  

Try this

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Jacked''' are you saying to try the tone and naptha before basing?


  "I'm not really here "  

 

 

 

 

 

 

geezmeister
(Bee of the Month)
09-27-02 10:31
No 361258

  

  

Me too!

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I'd appreciate some more details too, Jacked. I think you know more about something a couple of us have been toying with than you're telling us. This might solve a couple of questions SWIG's been trying to answer.


Mostly harmless

 

 

 

 

 

 

ChemoSabe
(Hive Addict)
09-27-02 10:49
No 361268

  

  

Special Request

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Also Jacked, if it's no inconvenience, I think it would be great if you could post the latest "state of the freebase address".

Swim's been looking over some of your older FB reaction postings and in one you state that the older ones needed an update to include new things you'd learned thru experience.

No problem if you can't get right to it but I'm sure there is a decent audience that would be interested to hear what your current FB reaction procedure is.

Thanks in advance,
CS


I've fallen into a bottomless pit and I can't get it up.

 

 

 

 

 

 

zibarium
(Naked)
09-27-02 11:16
No 361282

  

  

end product of fb rxn is the same as the HCl

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thought the rumour of otherwize should bee put to rest.

the rxn is different, to bee sure. and very well may allow a better yield than reacting the salt...if all else is the same. seems to bee more forgiving of marginal rp.

 

 

 

 

 

 

geezmeister
(Bee of the Month)
09-27-02 11:27
No 361287

  

  

Zib noticed it too

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Yep. It will run with a lower ratio of good red than a salt reaction will.


Mostly harmless

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-27-02 13:17
No 361345

  

  

lower ratio of good red

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ok now ya got me thinkin''' and that's hard to do ...
what would a good guess bee to the ratios for rp:?

SWIHFT is working on another trial run with tetra as a wash just to see if it makes a difference..

He still wants to see if the overnite basing played a role in higher yeilds so he's doing the same thing with this trial run...

  cool


  "Go ahead jump  "  

 

 

 

 

 

 

VideoEditor
(Hive Bee)
09-27-02 17:22
No 361425

  

  

Perception

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The quality or kick of the end product is a direct result of the body chemistry that occurs after absorption. By-products and other toxins usually present in d-meth, inter fear or change how the body chemistry works. The perception that the free base product is stronger is because when properly produced, the free base product is cleaner, containing less or different contaminants. Pure d-meth from HCL and from free base are chemically identical.

SWIVE is hard at work on Straight to Bee II. A simplified version with higher yeilds. Stay tuned...


Real Men Don't Preview Their Edits

 

 

 

 

 

 

VideoEditor
(Hive Bee)
09-27-02 18:14
No 361446

  

  

and quality

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SWIVE's dog makes these from free base.


Real Men Don't Preview Their Edits

 

 

 

 

 

 

handsfull2
(Hive Bee)
09-27-02 18:22
No 361449

  

  

'and quality'

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Hell VE'''' I'd show them puppies off tooooo......

Now quit playing and get us more info on the universal phase two okie dokie;;;;;; oh I just started a animal shelter for puppies ;;; send as many as you like....... cool


  "Go ahead jump  "  

 

 

 

 

 

 

zibarium
(Naked)
09-27-02 19:50
No 361472

  

  

an explanation...not a diss

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v.e. i'm sure knows this, and will take no offense...

but as far as lurid, center-fold pics of crystals go:

these can bee had thru extensive re-crystalizations...no matter how you did the rxn; and even if the yield sucked ass.

zib needed to squelch the implication that the end product would bee different, once it looked like that pic.

though the journey to it can certainly vary alot, as per yield, and amount of hassle.

it is possible to obtain a large crystal of meth thru the funkiest of rxns, with crappy equipment , non-dried solvents, no ph paper, and marginal precursors. but it will bee an effort...and lousy yield.

 

 

 

 

 

 

geezmeister
(Bee of the Month)
09-27-02 20:30
No 361488

  

  

Zib--true, but...

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Zib...that is true...but when you get those large crystals so soon and with so little effort, when the stuff just absolutely wants to give these to you...you know you are getting it right from the start and know that you have the stuff that's as good as it gets. Growing crystals is much easier when you stuff if high quality and clean to start with.

VE: Very pretty crystals, and very clear. Nice work!


Mostly harmless

 

 

 

 

 

 

Jacked
(Ancient Alchemist Delux)
09-28-02 01:15
No 361560

  

  

Do you think that I would settle for second best?

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Swim says he hasn't seen any product better than his and after recrystilizing there is some that looks as pretty but just doesn't have the kick.. If it is an impurity I say we start manufacturing that impurity by it self.. Larger amounts of acetone disolves more crap and loosens everything nicely, the naptha starting at room temp pulls a silt looking material and clouds up, decant this off before it has time to settle, keep washing with the naptha each time adding heat, it don't haft to boil, do this until it does not cloud up on you. Go back to a final acetone wash with a liberal amount and vacuum filter or layout on cookey sheet. Swim says the 70 to 75% of off orange pseudo laying there can be based for FB reactions or strait into the flask as an Hcl....The post reaction solvent is the key, It's always the same type solvent that washed the pseudo. Might mean nothing but Swim  thinks it could be a solvent solective issue that yields 65 to 70% of top notch gear eaving the crap behind.    
Some of you might be underestimating the cleaning powers of a highly consentrated Hi/Rp reaction as well as the reducing that goes on.. I do believe in the old saying "shit in shit out" and do not advacate pill chunking.. So the cleaner the better by all means, pay them dues...I sure did.


The end result is directly connected to the effort applied

 

 

 

 

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