Cal
August 15th, 2001, 05:46 PM
hi i'm new here i just came here via the link that the real put up on the site totse
uhm i was wondering if this is true info cause now that the real's gone we have no mod and noone knew as much as he did so i was wondering if any of you guys could tell me if it's true or not.
Here Is How To Make Hydrazine..
Prepare a solution of 1500 mL of 28-29% ammonium hydroxide, 900 mL of water, 375 mL of 10% gelatin solution, and 1200 mL of normal sodium hypochlorite solution. It is absolutely imperative to use distilled water, the presence of any contaminant ions will screw up this reaction! It is possible to use starch, glue, or glycerol instead of gelatin, but they are inferior. Mix these chemicals in a large glass dish, like a pie plate or bowl, or just use several portions, as this is nearly a gallon of liquid. This mixture is heated as rapidly as possible and boiled down to one-third of its original volume. The solution is then cooled thoroughly with ice and suction filtered twice to remove any impurities. When filtering, first use towels (like a washcloth), then use regular filter paper on top of some cloth (like from a T-shirt).
The resulting liquid is dilute hydrazine hydrate. To make concentrated hydrazine hydrate, mix 144 mL of dilute hydrazine with 230 mL of xylene in a round-bottomed 500-mL Florence flask. Fractionally distill the mixture in an atmosphere of nitrogen, the xylene will first pass over with most of the water, then the hydrazine will pass over. Keep the fractions separate of course. The resulting hydrazine hydrate will be 90-95% hydrazine. This concentration procedure is meant for 60% hydrazine hydrate, since the hydrazine hydrate prepared above may be greater or less than 60%, some experimentation may be needed to find the proper amount of xylene to use (more xylene is needed for dilute hydrazine, less for more concentrated hydrazine).
To obtain anhydrous hydrazine, mix 20 g of potassium hydroxide per 100 g of >90% hydrazine hydrate in a beaker, let this mixture stand overnight so much of the water can be withdrawn. After standing, filter the solution to remove the hydroxide. Add to the filtered liquid an equal amount by weight of sodium hydroxide. Place this mixture in a round-bottomed 500-mL Florence flask, reflux for 2 hours, then distill in a slow stream of nitrogen. You must use nitrogen, distillation in air may lead to an explosion!
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I like pot guy, and i'm hungry guy yea!
uhm i was wondering if this is true info cause now that the real's gone we have no mod and noone knew as much as he did so i was wondering if any of you guys could tell me if it's true or not.
Here Is How To Make Hydrazine..
Prepare a solution of 1500 mL of 28-29% ammonium hydroxide, 900 mL of water, 375 mL of 10% gelatin solution, and 1200 mL of normal sodium hypochlorite solution. It is absolutely imperative to use distilled water, the presence of any contaminant ions will screw up this reaction! It is possible to use starch, glue, or glycerol instead of gelatin, but they are inferior. Mix these chemicals in a large glass dish, like a pie plate or bowl, or just use several portions, as this is nearly a gallon of liquid. This mixture is heated as rapidly as possible and boiled down to one-third of its original volume. The solution is then cooled thoroughly with ice and suction filtered twice to remove any impurities. When filtering, first use towels (like a washcloth), then use regular filter paper on top of some cloth (like from a T-shirt).
The resulting liquid is dilute hydrazine hydrate. To make concentrated hydrazine hydrate, mix 144 mL of dilute hydrazine with 230 mL of xylene in a round-bottomed 500-mL Florence flask. Fractionally distill the mixture in an atmosphere of nitrogen, the xylene will first pass over with most of the water, then the hydrazine will pass over. Keep the fractions separate of course. The resulting hydrazine hydrate will be 90-95% hydrazine. This concentration procedure is meant for 60% hydrazine hydrate, since the hydrazine hydrate prepared above may be greater or less than 60%, some experimentation may be needed to find the proper amount of xylene to use (more xylene is needed for dilute hydrazine, less for more concentrated hydrazine).
To obtain anhydrous hydrazine, mix 20 g of potassium hydroxide per 100 g of >90% hydrazine hydrate in a beaker, let this mixture stand overnight so much of the water can be withdrawn. After standing, filter the solution to remove the hydroxide. Add to the filtered liquid an equal amount by weight of sodium hydroxide. Place this mixture in a round-bottomed 500-mL Florence flask, reflux for 2 hours, then distill in a slow stream of nitrogen. You must use nitrogen, distillation in air may lead to an explosion!
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I like pot guy, and i'm hungry guy yea!