Log in

View Full Version : Preparation of diethoxynitramine dinitrate - Archive File


megalomania
June 17th, 2003, 08:10 PM
Cipolla
New Member
Posts: 37
From:
Registered: MAY 2001
posted 06-03-2001 07:09 PM
--------------------------------------------------------------------------------
Take 10 ml fuming nitric Acid, add about 2 - 3g Diethanole amine while cooling. Then bubble dry hydrochloric acid trhough the mixture and pour it after allowing to stand for a few hours into 20 ml acetic anhydride. Let again react for a hour or more and then pour the mixture into carbonate solution. A white solid should precipitate, this is diethanolnitramine dinitrate or (see subject). This coumpound is rather stable, will burn fast if exposed to flame and detonate readily if initiated. Lead block test is comparable to RDX. The "soil expansion test" I carried out using an amount of 5g offered a 20-cm-cater that was about 15 cm deep......


frostfire
Frequent Poster
Posts: 266
From:
Registered: SEP 2000
posted 06-03-2001 07:48 PM
--------------------------------------------------------------------------------
source, reference, patents.....please?
otherwise it's a big congrats for an inventor

sounds good except for the acetic anhydride, any substitute?



Cipolla
New Member
Posts: 37
From:
Registered: MAY 2001
posted 06-04-2001 11:15 AM
--------------------------------------------------------------------------------
That's no invention, its a well known explosive. You can find it in almost every literature about explosives.
I don't believe that there's a substitute for acetic anhydride.

P.S.: Don't try to invent anything. I had many explosives in mind from which I thought they would be very good and yet not known. Finally I found them all in the books about explosives.....
Like trimethylolaminomethane tinitrate, Monoethaholamin dinitrate, tartraic acid dinitrate, triethanolamine tetranitrate, Methylnitramine, Trinitropyridine.....



frostfire
Frequent Poster
Posts: 266
From:
Registered: SEP 2000
posted 06-04-2001 03:30 PM
--------------------------------------------------------------------------------
true, I've had this dream many times....
I believe there's or will be stronger explosive than thermonuclear (aka H-bomb)
that's one of my (dream) goal in physics research


CodeMason
Frequent Poster
Posts: 383
From: Your Nightmares
Registered: NOV 2000
posted 06-04-2001 06:12 PM
--------------------------------------------------------------------------------

quote:
--------------------------------------------------------------------------------
bubble dry hydrochloric acid
--------------------------------------------------------------------------------

It's only called hydrochloric acid when it's dissolved in water. As a gas, it is hydrogen chloride (anhydride).