benzo wacker salt washes?

[alkadelic]

In step 10. says wash ketone/dcm with sodium bicarbonate in water.(500ml each wash). how much sodium bicarbonate do i add??
In step 11. how much sturated NaCl do i add to(400-500ml) how much water??thanks...

[silenziox]

It's usually good to saturate the solvent with something..
So, dissolve sodium bicarbonate to water until it doesn't
dissolve anymore... Decant or filter to get rid of the solids.

[pooky]

Also use hot water to start,add in way too much and stir the hell out of it.But when making NaOH,use cold water as the reaction is quite exothermic.

[Just4Fun]

A saturated solution is simple. Add as much solid to the solution as it take until no more dissolves.  When no more solid will dissolve remove the excess.