dcm, toulene, methanol

[racemic]

oops chromic, my bad, there is something in the merck about boiling points of different methanol water soln's. Anyways you can't get dry methanol by distillation.

[Chromic]

You can get virtually dry MeOH by distillation. However, you require a very, very long column and a careful, slow distillation to properly separate it from water (400mm at the least)... and a very accurate thermometer.

Yeah, MeOH is miscible with DCM and with toluene and with DCM/toluene. And water is miscle with MeOH. But MeOH/DCM/Toluene/water will form two layers. One with mostly water, some DCM, some toluene.. the other with mostly DCM and toluene and some water.

[Prdy2GO]

Take some and add water and a drop of food coluring. Then add a fuck of a lot of salt (the plain kind) shake and let it settle you will ger 3 layers. You can figure it out from there...
Don't look at me I didn't do it!