Author Topic: Prep of NaI  (Read 3899 times)

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Chemikaze

  • Guest
Prep of NaI
« on: August 25, 2001, 08:30:00 AM »
Hey,

Vanillin can be iodinated in an aqueous solution of sodium triiodide (NaI3.NaI), made in situ from sodium iodide and iodine, forming 5-iodovanillin. - quote from iodovanillin.htm

So i`ve got almost everything for this reaction,the only problem is how to prepare NaI ?

As what is written there, there is an option of using chlorine and NaCl
but i dont wanna have "good" time with Cl when i can spare it with I :)
Any ideas?
BTW, i searched Hive - nothing found....
Thanks. ::)

Everybody in the house with a half an ounce
Not weed I meant coke dumb ass sit down!

jim

  • Guest
Re: Prep of NaI
« Reply #1 on: August 25, 2001, 08:39:00 AM »
NaI is sold in pure form at chem stores.  It is also sold as in Horse SHops for hoofing.

It is also in Iodized salt, although only in small amounts.

NaI is soluble in acetone, whereas NaCl is not...

Chemikaze

  • Guest
Re: Prep of NaI
« Reply #2 on: August 25, 2001, 04:15:00 PM »
Unfortunately i`m not from USA and i`m looking for some MAKE_IT_YOURSELF ways:) sorry to say :-[
thanks anyway

Everybody in the house with a half an ounce
Not weed I meant coke dumb ass sit down!

Agent_Smith

  • Guest
Re: Prep of NaI
« Reply #3 on: August 28, 2001, 04:12:00 PM »
This has been covered before, it can't be done very easily, especially starting from I2

blah blah blah something clever blah blah blah