News:

Registration doesn't require a real email.
Monero Donation Address: 897ESh4QoJgEytJueBPULziMDfNMToXkGMrvtUCJRo2NQRv2CXACHnmEzeMTkwQhnfcZsAc3ctXp6GsedhMfBv983rn5i84

Main Menu

Aniline synth???

Started by TripleXtacy, September 19, 2001, 10:01:00 AM

Previous topic - Next topic

0 Members and 1 Guest are viewing this topic.

TripleXtacy

A friend of swims who likes to play with fentanyl, has recently encountered a stumbling block. Due to new obstacles recently imposed in his area in regards to acquisitions of aniline have led him to discover new methods of possession.
His question is, has anyone experimented with the production of aniline via hydrogenation of nytrobenzene with Iron turnings/fillings?
If not has anyone got any tips as he is ready to give it a try anyways.
Thanks for your time.

The only secrets are the ones that keep themselves.

Rhodium

Yes, and it is an easy reduction. Look in the file

https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.txt

for general directions.


Rhodium

Yup, 300 documents HTMLized so far, 100 to go.

PrimoPyro

Can also be made by reaction of benzamide with hypochlorite salts. Another easy reaction, and Cheapskate used the same principle for his Anthranilic acid synthesis, from phthalic acid.

                                                    PrimoPyro

PolytheneSam

From what I remember the process in J. Gen. Chem. is electrochemical. 

Post 199874 (missing)

(PolytheneSam: "Re: Oxidative amination of an alkene, maybe an electro possiblity.", Chemistry Discourse)


http://www.geocities.com/dritte123/PSPF.html
The hardest thing to explain is the obvious

hellman

Benzene-nitrobenzene`````h2so4
nitrobenzene-anilin''''''zn/hcl or sn/hcl
If you want the procedure step by step just ask,.
It is also from vogels pract