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vaccume induced crystalization

Started by Vibrating_Lights, February 10, 2002, 01:46:00 AM

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Vibrating_Lights

If one were to have some freshly distilled, weighed freebase in a recieving flask,  could one not simply add the equimolar ammount of 38%Hcl  then stir under vaccume to induce crystylazation with further desication of the product.
Vl_

LaBTop

Some parts of your freebase will certainly not like you and leave.
You will need a solvent to dilute your acids in, to safely form your salts. LT/

WISDOMwillWIN

Chromic

Have the freebase in a non-polar, extract with acidic water (until pH 4), then boil off the water. Don't add concentrated HCl to your freebase.

Vibrating_Lights

Those md s that make the red colors Lt_
Ether is the choice.
Terbium you were right.
Ice bath on the gassing flask ensures 0 solubility of the HCL salt.
VL_