24 h ago swim starts his first lwr dream , after 4 month of reading....
it starts with 1:1,2:0,5:0,8 (e:LGI:LGRP:dH20). First mixed e+rp+dh20, then fixed a 40cm west-condenser on his 250 rbf. then let fall 4 portions of iodine through the condenser. magnetic stirbar mixed it well a litte white smoke was visible. after a few moments the flask was clear again and the ballon become little inflated.
then turned heat on till 98° C inside the flask was reached. little bubbles are visible and a nice slow reflux
(2 drops/min.) is going on. everything o.k. so far.
after 12 hours of refluxing first HI cryst. appears in the condenser. after 20 hours the ammount of HI cryst. is very high, so swin decided the wash this crystals down with 1ml of dh20. after this, a thin fog appears. this fog "circulates" in the flask, falls out of the condenser,
goes up and down..., ballon is unchanged.
Here comes the point where swin needed some advice:
now (after 24h)there is a very low rate of bubbling avtivity and refluxing (1 drop/minute).
swim plans to go for 48 hours, but what should he do now???
add a additional gram of iodine and some water? or better do nothing ?
there is no change of volume visible and the size of the bubbles is unchanged.
what is a shure sign, that the reaction is done?
thx