He bees,
This is no dream nor fantasy or a lie,but a tested syntheses route with a 95% yield!
It goes as follows:
In 2000 ml dry Methanol is dissolved 50 grams of tryptamineHcL,followed by 47,5 ml sodiummethoxide 30% in MeOH,58.8 gram of aceticacid 100% and as last 31.4 gram of
sodiumcyanoboronhydride.
The mixture is stirred with a magnetic stirrer and cooled with an ice-salt bath back to -2°C.
when it reaches this themperature there is dropped to this solution a mixture of 57.5 ml folmaldehyde 37% in 625 ml dry methanol in 30 minutes time.
After this the whole is stirrer for at least 1-2 days at 10°C by putting the whole in the refrigerator.
After this the reactionmixture is deluted by the same amound of water and made basic,pH 9-10,by adding a strong sodiumcarbonate solution to it.
hereby white particles precipitates which are filtered of and are washed with ethylacetate,which is combined later with the ethylacetate extracts.
the whole solution is distilled under vacuum as far as possible.
The residu is diluted with 3 liter of water,this solution is extracted 4-5 times with a total amound of 1.5 liters of ethylacetate which is combined with the earlyer extract.
the ethylacetate solution is dryed with anhydrous magnesiumsulfate,which is wetted with fresh ethylacetate.
The whole is filtered and the ethylacetatesolution is distilled down to circa 100-150 ml under vacuum.
this is put in a small beaker and put in the freezer for a day.
yield 45.4 gram yellow-colored DMT (95%)!!!
