Swibs been doing this for awhile, and honestly average 50% yeilds everytime. Swibs was just happy with that.
Its the rp/i/e long wet reflux, about 10 grams each time.
When swibs done an acid/base he always use hot Dh2O and NOT HEATED mineral spirits. Should swib heat the mineral spirits also, making both polar, and non-polar liquids heated?
Swib uses both freebase crystals and hcl form and doesnt know how heating both liquids would affect each type of pseudo?
Swibs asking because Swibs been reading here about heating Naptha for an A/B. But theres no mention of mineral spirits.