The Vespiary

The Hive => Stimulants => Topic started by: auntyjack on January 29, 2004, 06:52:00 PM

Title: Regarding the volatility of ephedrine
Post by: auntyjack on January 29, 2004, 06:52:00 PM
just hypothetically now, if someone had about one litre of water with a few grams of ephedrine freebase disolved in it, and then this someone evaporated the water to dryness under a condenser, collecting the water, would any of the ephedrine vaporise with the water or would it have to be steam distilled?

Title: the ephedrine would distill over with the...
Post by: Xicori on January 29, 2004, 08:50:00 PM
the ephedrine would distill over with the water - it is steam volatile!

just add HCl until the solution is slightly acidic before evaporation - Ephedrine.HCl isnt steam volatile any more!

Or Extract the water with a NP and evaporate this to get the base!