Author Topic: Preparation of LSD with Thionyl Chloride  (Read 11118 times)

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Rhodium

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It was actually lugh who retrieved theĀ ...
« Reply #20 on: February 10, 2003, 05:56:00 AM »
It was actually lugh who retrieved the article, I just hosted it.

You have gotten it all wrong, they say they are condensing the structure IX with the hydrochloride salt of lysergic acid chloride using chloroform/tributylamine as solvent. There are also talk about making the acid chloride with oxalyl chloride and then something about making the acylazide with NaN3 - some german bee migh shed some light on this.