https://www.thevespiary.org/rhodium/Rhodium/worlock/rxn1.html#rati (https://www.thevespiary.org/rhodium/Rhodium/worlock/rxn1.html#rati)
Is there a formula that is "set in stone" on the amounts of RP/I/E/DH20 that should be used? The only constistancy in the formula is that at some point in time, they all are put in a flask.
Post 449625 (missing) Post 478526 (https://www.thevespiary.org/talk/index.php?topic=8238.msg47852600#msg47852600) Post 467035 (https://www.thevespiary.org/talk/index.php?topic=7947.msg46703500#msg46703500) Post 487707 (https://www.thevespiary.org/talk/index.php?topic=7927.msg48770700#msg48770700)
Nothing engraved in stone. There are any variety of ratios that will fit within the envelope of success. I have mentioned these ratios and discussed their relationships to each other in a few posts:
I will say this much about the ratios you use: You are using far too much iodine. You are losing yield using that much. At the size reaction you are doing 1:1 ratios of I:E will be sufficient; you never need to exceed a 1.2:1.0 ratio of I:E except maybe in nano reactions.