Author Topic: TS@ #2 rxn reduction time.
Arthur Bach
Member posted 10-23-98 02:51 AM
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I don't think I really belong in this forum yet, but the other Bees refered me here for a posibble answer to this question.
If someone was to follow TS2 and scale up #2 5x, can the rxn be performed at 60-70c with a 6 liter three necked flask, reflux condenser and thermometer to reduce the rxn time ? Is there another way to reduce the stirring sime ?
Arthur Bach
Member posted 10-25-98 06:58 PM
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Aparrently no one knows. Does anyone have a ideas to reduce the rxn time from 72 hours ?