The Vespiary

The Hive => Novel Discourse => Topic started by: LSDforTHEfreaks on July 27, 2002, 04:53:00 AM

Title: Safrole + IH ---> Iodosafrole
Post by: LSDforTHEfreaks on July 27, 2002, 04:53:00 AM

I chill safrole for 48h with 70% HI(2degrees) then I have Iodosafrole. Is that right?

Sorry my english is bad.

Title: Halosafrole technique.
Post by: Anansi on July 28, 2002, 02:18:00 AM

One of the best ways to halogenate safrole is by the use of DMSO and Sodium Halide with a little conc. sulfuric acid.

There is a wealth of information available on this proceedure, just UTFSE and also check out

https://www.thevespiary.org/rhodium/Rhodium/chemistry/halosafrole.txt (https://www.thevespiary.org/rhodium/Rhodium/chemistry/halosafrole.txt)

Hope this helps,

...Anansi