Author Topic: Safrole + IH ---> Iodosafrole  (Read 2291 times)

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LSDforTHEfreaks

  • Guest
Safrole + IH ---> Iodosafrole
« on: July 27, 2002, 04:53:00 AM »
I chill safrole for 48h with 70% HI(2degrees) then I have Iodosafrole. Is that right?

Sorry my english is bad.

Anansi

  • Guest
Halosafrole technique.
« Reply #1 on: July 28, 2002, 02:18:00 AM »
One of the best ways to halogenate safrole is by the use of DMSO and Sodium Halide with a little conc. sulfuric acid.

There is a wealth of information available on this proceedure, just UTFSE and also check out

https://www.thevespiary.org/rhodium/Rhodium/chemistry/halosafrole.txt



Hope this helps,

...Anansi