WOW
Thermal seperation is *REALLY* the way to GO!!!
Let me give all of you the run down on what I've done tonight!
Used the Rhodium synth for Hexamine tablets to Methylamine.
Step one
I added my water, acid and dropped in my hexamine tablets.
Step Two
Allowed to mix together and the Hexamine tablets wore away
to nothing. After everything was dissolved I heated the
mixture until no more carbon dioxide bubbles came out.
Step Three
I noticed that the Ammonia crystals were forming, I put the
jar into the fridge. Then a huge amount og crystals formed
after like 5 minutes... just let it sit it's not going to
freeze like plain water would. Then after it seems like
nothing else will settle out (15 min) you can get out the
methylamine by using a medical syringe. It's so fine that
the tip acts like a filter. Let that syringe sit in the
freezer for like 5 minutes. Notice that the syringe has
no crystals of Ammonia! You have methylamine!!! Of course
you will need to get rid of that damn water. Use Rhodiums
idea of dessicating... Use damp rid from the local hardware
store. It's more hydroscopic than methylamine. So it
pulls the water onto itself. Think of Damp Rid (Calcium
something .... im tired) as a bully snatching a lollypop
(the water) from a little kid (the methylamine) So after
a while you just have a little kid (methylamine)
((( re-edit after the fact : I got tired of waiting for
my piece of shit calcium dissector and I whipped out
a burner and cooked that shit up... its was of high quality
just get a portable propane burner and cook that shit up
OUTSIDE WITH GLASS! Methylamine Hcl fucks up Metal.
It turns purple (im pretty sure) I fucked up a metal spoon
that way.))))
So there.. no solvent used at all... a 100% thermal
seperation. Go save your solvent for other things
This works way faster too!!!
Maybee I should be called the "Speed Bee"
for making it faster
Gott Mit Uns!