Author Topic: Aniline synth???  (Read 2604 times)

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TripleXtacy

  • Guest
Aniline synth???
« on: September 19, 2001, 10:01:00 AM »
A friend of swims who likes to play with fentanyl, has recently encountered a stumbling block. Due to new obstacles recently imposed in his area in regards to acquisitions of aniline have led him to discover new methods of possession.
His question is, has anyone experimented with the production of aniline via hydrogenation of nytrobenzene with Iron turnings/fillings?
If not has anyone got any tips as he is ready to give it a try anyways.
Thanks for your time.

The only secrets are the ones that keep themselves.

Rhodium

  • Guest
Re: Aniline synth???
« Reply #1 on: September 19, 2001, 10:06:00 AM »
Yes, and it is an easy reduction. Look in the file

https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.txt

for general directions.

Bwiti

  • Guest
That text doc was HTMLized to http://www.rhodium.
« Reply #2 on: June 05, 2002, 01:41:00 AM »
That text doc was HTMLized to

https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.cheapskate.html

8)

Love my country, fear my government.

Rhodium

  • Guest
Yup, 300 documents HTMLized so far, 100 to go.
« Reply #3 on: June 05, 2002, 01:46:00 AM »
Yup, 300 documents HTMLized so far, 100 to go.

PrimoPyro

  • Guest
Aniline
« Reply #4 on: June 05, 2002, 01:49:00 AM »
Can also be made by reaction of benzamide with hypochlorite salts. Another easy reaction, and Cheapskate used the same principle for his Anthranilic acid synthesis, from phthalic acid.

                                                    PrimoPyro

PolytheneSam

  • Guest
From what I remember the process in J. Gen. Chem.
« Reply #5 on: June 05, 2002, 03:15:00 AM »
From what I remember the process in J. Gen. Chem. is electrochemical. 

Post 199874 (missing)

(PolytheneSam: "Re: Oxidative amination of an alkene, maybe an electro possiblity.", Chemistry Discourse)


http://www.geocities.com/dritte123/PSPF.html
The hardest thing to explain is the obvious

hellman

  • Guest
very easy
« Reply #6 on: June 19, 2002, 03:10:00 AM »
Benzene-nitrobenzene`````h2so4
nitrobenzene-anilin''''''zn/hcl or sn/hcl
If you want the procedure step by step just ask,.
It is also from vogels pract