"ALL the bullshit that Baalchemist posted about 1 gallon jugs and seed crystals and putting the jugs upside down and draining off liquid is BULLSHIT.
I tried that. The liquid is formed ON TOP of the crystals, not on the bottom. If you turn the jug upside down and crystallize, none of the liquid will pour out--you will have to drill a hole in the bottom of the jug to drain the liquid and then cut the jug apart to get the crystals out. There is NO WAY he actually did it the way he describes--he just made that bullshit up. Not one bee posted it right. It is SO FUCKING SIMPLE, I can't believe it. The natent liquid is forced to the top and middle of the 20L bucket by the crystal growth on the bottom and sides of the bucket, so the most simple decantation by pouring off the liquid is all that needs to be done. It is not necessary to check temperatures and do many decantations at 2 to 5 degree intervals, since the unwanted product does not crystallize at above -9 C, which is about as cold as a second hand deep freeze is going to get, in fact you DO NOT want a super-duper freezer, just an old one that can cool to -5 C. Some other bee mentioned filtering the crystals--BULLSHIT! All that is needed to achieve d20 of >1.099 is 3 times crystallization and simple decantation. Nothing else. For most people, 2x crystallization which gives d20 of >1.098 will be sufficient.
Fuck, it makes me mad to realize the amount of time I wasted on fractional distillation !
The only drawback to this method is that it takes a few days. But shit, fuck, damn! If I had known how simple it was, I would have done it already a long time ago.
And if I hadn't tried out Baalchemists' BULLSHIT post, I wouldn't have spilled crystalls all over the floor when I cut the jug open, so that now the whole fuckin place reaks of safrole!
ForYourInfo the density of 100% safrole is probably close to 1.100, because simple 3x crystallization gives me a clear liquid with d20 of 1.0994. The d20 is definitely NOT 1.096 like has been posted by everyone on Hive, including you (LT/) and terbium.
All of this makes me wonder about the mentality of bees who inhabit Hive. Baalchemist, for example. What was he thinking, what was his possible motive, when he posted that BULLSHIT about 1 gallon jugs and seed crystals and turning the jugs upside down overnight in freezer. I tell you he NEVER actually did what he posted, because it is PHYSICALLY IMPOSSIBLE. Who are these weirdos, who pose as cooks, but obviously make things up. What is their fucking motivation? And am I the only idiot who actually TRIES what others post? Fuck, I'm mad.
If I were still posting, I would post a scathing write-up about separating safrole from sassy, and I would flame every single bee who ever once mentioned fractional distillation of sassy, then I would roast Baalchemist for being a blatant liar about those fucking upside down jugs, and then I would burn anybody who ever got the d20 of safrole wrong, and then probably call into the question the motivation of all those bees who post bullshit, and name them, one by one. Baalchemist, youAxxxxx Mxxxxxxxxxx. And I'm stone sober, btw."
Its quite interesting to stumble across a thread 6 months later such as this one. These are the type of people that blame all their inept behavior, stupidity & grossly undersized genitallia on anybody else other than their own inbred, downs-syndrome infested gene-pool. I bet he can type at least 70/wpm with one hand, while he's feverishly stroking his life-long inadequacy with the other. You should have just shoved the upside down jug up your ass, & then execute a handstand in your freezer, then you could've just spit out the non-safrole components along with all that other shit that seemed to be coming out of your mouth. If he was such the intellect he claims, why did his safrole end up all over the floor then?
(hint) because he's an idiot maybe, or possibly he could'nt perform the task one-handed..............