Terribly sorry for the lack of details gentlemen.
SWIM was extremely happy with yeild considering the post performic mix mis not orange colour as supposed to be, not even brown, it was black. SWIM postulated that it was due to using 50% H2O2 (calculated to use a smaller amount) and not adding water to dilute it.
Rhodium;
Yeild was calculated by weight and is from iso->MDP2P. Glycol was not actually weighed, just assumed there was about 1kg from 1kg of iso. Methanol was not used, due to volume restrictions of the 5L flask. Acid was preheated to 80c (This allows time to play with heat settings until you know it will hold 80c for a given volume) and then the still luke warm (assumed) glycol added. it was then mag stirred on a heating mantle and held at 80c for the 5 hours.
abacus;
SWIM thought it was a forgone conclusion that the Hcl hydrolysis worked, so SWIM went with it. As for amination, due to lack of experience (2nd time) it was split into several portions/reactions. Following Os's writeup on Rhod's page, first portion yeilded about 50%, second portion yeilded 95+%, third portion yet to aminate.
So "works as usual", SWIM wouldn't know, but it sure works! Yes, it was tested!