Swim is working on the MDP2POL oxidation working with diffrent combinations of conditions and solvents. 22 diffrent carefully planned, controlled monitered and recorded experiments each with only one variable are in order once all the nescesary information is collected in hopes that one of the 22 procedures will work, and work every time. In theory there is no problems with the procedure for a normal allaybenzene but with safrole acetic conditions combined with heat cause the rapid carbo cation rearrangement to the P1P diol. Swim is looking for a procedure that will safeguard againsed this rearrangement and produce a working synth to ketone using all Otc Percursers. Swim has been non stop working on this synth for the past couple of months and is busy doing many other things relating to this subject. He has looked for this data himself. Solvent solubilitys needed are , DMSO ACETONE METHANOL ETHER He will greatly appreciate all help in this effort and give the due credit to all those who came before him and to all those who are presently helping him. the Day is near when all of this will make sense. Now is that worth helping out in. He gaurentees it would definatly be worth any effort that is invested into the project by anyone. Hundreds of dollars have already been spent by many bees on the origional Procedure and thousands will be put into the rest until there is a solution. He sends his apologies to the sass gods about all the wasted sass althoug it could have not gone to any better purpose.
VL out
Thanks
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Hopefully will have the answers by christmas