Author Topic: how to separate P2P and amphetamine mixture?  (Read 2436 times)

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tropine

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how to separate P2P and amphetamine mixture?
« on: November 11, 2003, 06:07:00 PM »
So a P2P mixture of amphetamine is in DCM.  Yes one could use 20% HCl in water to wash the DCM with to removed the amphetamine but the concern is that the amphetamine wont "see" the protons since the HCl/water and DCM are not soluble.  Maybe just shaking the hell out of the DCM/HCl/Water mixture will be give the amphetamine sufficient exposure to the protons?

Bandil

  • Guest
Yes, that's how you generally perform A/B...
« Reply #1 on: November 12, 2003, 01:19:00 AM »
Yes, that's how you generally perform A/B workup. Shake the hell out of that baby, and you'll have your material in the water phase!