Author Topic: Sodium Triacetoxyborohydride Reductive Amination  (Read 2269 times)

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chinone

  • Guest
Sodium Triacetoxyborohydride Reductive Amination
« on: September 24, 2002, 09:10:00 AM »
Has anyone tried this? If so what were the results and conditions used?

Organikum

  • Guest
yes. daily between 8:30 and 9:00 am. why ask?
« Reply #1 on: September 24, 2002, 11:14:00 AM »

http://www.callery.com/pdf/bulletin/calselect_stab.pdf



under "applications" is listed what this compound maybe used for.

ORGY

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slappy

  • Guest
Triacetoxy has been used, and was found to giveĀ ...
« Reply #3 on: October 02, 2002, 07:20:00 PM »
Triacetoxy has been used, and was found to give very favorable results.

1 eq. NaBH(OAc)3 in 47.5/47.5/5 Dichloroethane(DCE)/THF/AcOH and amine freebase.