Author Topic: drying aceton and ethyl alcohol  (Read 4439 times)

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Pijotr2k2

  • Guest
drying aceton and ethyl alcohol
« on: December 08, 2002, 04:46:00 AM »
short question :)
what is the easiest method to dry aceton and ethyl alcohol (ethanol)?


demorol

  • Guest
Short answer: UTFSE! I'm sure this question has ...
« Reply #1 on: December 08, 2002, 05:05:00 AM »
Short answer: UTFSE!

I'm sure this question has been answered before.

I'm dreaming of the white crystals.

Barium

  • Guest
UTFSE
« Reply #2 on: December 08, 2002, 06:47:00 AM »
How dry do you want them? 1 ppb water or 5% water? You need to be a tiny bit more specific.

Catalytic hydrogenation freak

Pijotr2k2

  • Guest
sorry but i have really no nerve on spending ...
« Reply #3 on: December 08, 2002, 10:28:00 AM »
sorry but i have really no nerve on spending whole days on reading every match given in the FSE for answers.
my only question is, how to dry aceton and ethyl alccohol for using them e.g. in a recrystallisation.

odin

  • Guest
Speed question
« Reply #4 on: December 08, 2002, 10:35:00 AM »
On Rhodium site you can find these inf. for less then 2 mins

Pijotr2k2

  • Guest
ok thank you VERY much for your GREAT help !!
« Reply #5 on: December 08, 2002, 10:42:00 AM »
it was a short question which normally requires only a simple short answer -> not at least ONE really usefull one came from you--- sure a GREAT forum here, but ignorant dumbasses of users who ruin this all!

demorol

  • Guest
Process for drying ethanol and acetone is written ...
« Reply #6 on: December 08, 2002, 12:13:00 PM »
Process for drying ethanol and acetone is written in Vogel's Textbook of Practical Organic Chemistry, 3rd ed. You can find it on Rhodium's page.


I'm dreaming of the white crystals.

odin

  • Guest
Flame
« Reply #7 on: December 08, 2002, 12:17:00 PM »
You will sure get it, you ask for it! :P

odin

  • Guest
And
« Reply #8 on: December 08, 2002, 12:21:00 PM »
>thank you VERY much for your GREAT help
Yore welcome! :P

RepVip

  • Guest
sure a GREAT forum here, but ignorant dumbasses ...
« Reply #9 on: December 08, 2002, 01:09:00 PM »
sure a GREAT forum here, but ignorant dumbasses of users who ruin this all!

It's motherfuckers like you that ruin the hive's spirit. Cluttering up the forums with stupid as shit questions. You're the ignorant one. It's annoying as hell to see the same fucking questions over and over. Get a fucking clue. It's not enough you're a fucking dumbass, asking pathetic questions, but you have an attitude, getting on here telling us our business? Get-FUCKING-lost!
Us? Ignorant? We go out of our way to help stupid ass people like you - BUT FIRST YOU HAVE TO HELP YOURSELF. Nobody responds to stupid fucking questions like yours... it's just a waste of time.

pickler

  • Guest
Short simple answer. Dry out epsom salt in oven ...
« Reply #10 on: December 08, 2002, 01:48:00 PM »
Short simple answer. Dry out epsom salt in oven for about an hour or so on 350f. Put dried epsom in your acetone or whatever you want to dry. Repeat 2 more times. This answer is in the search engine and over at rhodiums. Try doing a little searching before asking questions that have been covered numerous times.

I went into the business for the money, and the art grew out of it.-Charlie Chaplin


PolytheneSam

  • Guest
CaCl2 for acetone and CaO for alcohol.
« Reply #11 on: December 08, 2002, 03:57:00 PM »
CaCl2 for acetone and CaO for alcohol.  Alcohol (ethanol) is very hydroscopic.  Salts that form hydrates are not good enough for drying alcohol.  You need something that reacts with water like CaO.  Download Vogels from Rhodium's page.

http://www.geocities.com/dritte123/PSPF.html


The hardest thing to explain is the obvious

Barium

  • Guest
Hey!
« Reply #12 on: December 09, 2002, 03:24:00 AM »
You didn´t specify that you wanted them for recrystallisation. Hence I, had no idea how dry you wanted the solvents. If I had knew I would have answered you dry ethanol by azeotropical distillation with toluene and acetone by simple distillation.

What´s this attitude you´re showing because you didn´t get an answer within 10 minutes after your lazy ass managed to scribble the question? Instead of getting used to be spoonfed all information, why don´t you learn how to fucking find it yourself. Noone here will spoonfeed you anyway. 

Catalytic hydrogenation freak