The Vespiary
The Hive => Methods Discourse => Topic started by: blaztoff on November 07, 2001, 07:52:00 AM
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Has anyone come up with a good suggestion on what to use for the DMF O2 Reaction Vessel? I have searched around and everyone seams to have Ghetto rigged with no clear winner on what to use. I have been researching talking to Glassblowers even yet no one really seams to Know. Plastic it seams will wear out. SS is a no go but for a 4L reaction Vessel nobody seams to know proper thickness and stuff. Anyone have an answer?
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Glass filter carboys are made of some of the thickest borosilicate you will find and they have held 3 atmospheres on a consistent basis. Plenty of reaction volume as well. Or just get a glasteel pfaulder 10 gallon RX-series w/ helical impeller... mmmmmmmmmmmm chem porn... ahhhhhh........
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carboys good idea didn't think of that one thanks. 3 atmospheres is how many psi? thanks
what are you goofy?
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thanks madmax a regular round bottom flask can't take that pressure. swim knows from experience. ::)
what are you goofy?
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if you want to scale up use a ss paint sprayer with overhead stirring, and included psi gauge. oh yeah use a hdpe bucket inside for reagents or you're fucked!
hope this helps
j
"fuck the media"
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Don't use the bucket inside. When it gets hot, the steam goes over the edge and you lose water.
Use this, teflon coated:
(https://www.thevespiary.org/rhodium/Rhodium/hive/hiveboard/picproxie_docs/000234167-file_q4py.jpg)
Free Strike too.
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The wacker will NOT work with very pleasing results if done in a stainless vessle, expect enough "tar" and shit to re-pave your driveway. As Grouch mentioned telfon coat that puppy and you should be fine...
::) ;D :) :P ;) Mean People Suck ;) :P :) ;D ::)