Author Topic: crystal oil  (Read 3038 times)

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losthope

  • Guest
crystal oil
« on: August 04, 2004, 10:55:00 PM »

evilscripter69

  • Guest
Gas in the pan?
« Reply #1 on: August 05, 2004, 12:49:00 AM »
Is  methane not a gas??  Did you mean Meth ?
 be more specific, what methods did you use, so on. Maybe then you might get help.

Methodicalman

  • Guest
crystal oil
« Reply #2 on: August 05, 2004, 02:07:00 AM »
take your oil,check ph,take one cup warm water,one spoon red devil lye,mix,and pour 1/2 the cup thru your oil,let settle and room temp,check ph again.you want 12 to 14 ph level;before gassing,which will be cut in 1/2 for product when u gas.,,,Before ph-ing...run an aquarium pump (airiate)your oil for a couple hours to get rid of gas.  Use salt and sulphuric, instead of A&M or A&H...better gas better control.On an R$B.,,the PH must be right to GAS  ,unlike shaker way...Humidity will kill any gas return also. 70 degrees with no more than 60% humidity., is ideal.[purple]

geezmeister

  • Guest
meth oil in a pan?
« Reply #3 on: August 05, 2004, 07:35:00 AM »
You should stir the meth oil in a suitable nonpolar solvent before gassing.


dextro

  • Guest
How much NP is the right ratio to dissolve the
« Reply #4 on: August 05, 2004, 10:25:00 AM »
How much NP is the right ratio to dissolve the FB before gassing ( ex. 20ml FB in ????ml Toluene) ?

After steam distilling of the FB, is then a (5%) NaOH wash recommendable (before H20 and brine) or is this overkill/nonsense?

only water/brine washes are enough?

thx