The Vespiary

The Hive => Chemistry Discourse => Topic started by: synthesys on March 18, 2003, 08:38:00 PM

Title: NH2OH + MDP2P -> R'N-OH +GAA+ Pd/C+H2 -> ?
Post by: synthesys on March 18, 2003, 08:38:00 PM

If you hydrogented an oxime of NH2OH/MDP2P, and the resulting oil had most of the properties of MDA freebase, but was not soluble in acidic water, then the reduction was not complete, than you have something like RNHOH instead of RNH2. How can I determine that? If it proves to be RNHOH, can I use NaBH4 to reduce it further?



Synthesys

Title: Fuck all that
Post by: Vibrating_Lights on March 19, 2003, 03:30:00 AM

reduce the oxime with aa/al/hg.  search anitbodys posts.  80%yeild