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Author Topic: Opps, grabbed the wrong can!  (Read 2503 times)

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DarkSky

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Opps, grabbed the wrong can!
« on: December 10, 2003, 06:39:00 PM »
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DarkSky

  • Guest
Is it possible to take the soultion, wash with
« Reply #1 on: December 10, 2003, 07:15:00 PM »
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jackhole

  • Guest
Let the acetone evaporate
« Reply #2 on: December 10, 2003, 08:12:00 PM »
Let the acetone evaporate and proceed as usual.  With a reaction that size, it should only take a few hours.

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energizer_bunny

  • Guest
Good advice...
« Reply #3 on: December 11, 2003, 09:58:00 AM »
Evap off the tone then do the wash...but!

All this was cooked on 99.5C for 3 hours and everything was going perfect.


Where is it written that a rxn under LongWetReflux conditions is going to be complete @ 3hours?
That calculation defy's scientific logic.



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