I've been away awile, so bear with me if someone has covered this before.
Patent US3365499
describes an "Improved Wacker" process whereby one adds the H2O AFTER the solvent, p-benzoquinone, palladium chloride and olefin have been mixed together, rather than adding the H2O upfront. The example given in the Patent claims a 12% increase in Ketone yield. Has anyone tried this or will I be the first to test this?
Also, if the favorite olefin is added all at once to the methanol, PdCl2, and p-benzoquinone, will that result in an exothermic reaction?
Thanks!