http://patft.uspto.gov/netahtml/srchnum.htm (http://patft.uspto.gov/netahtml/srchnum.htm)
Patent US4638094 (http://l2.espacenet.com/dips/viewer?PN=US4638094&CY=gb&LG=en&DB=EPD)
Post 107768 (missing)
(smokemouth: "MDP2P with PdCl2 and MeONO, 73% - sunlight", Methods Discourse)Post 107769 (missing)
(smokemouth: "Re: MDP2P with PdCl2 and MeONO, 73% - sunlight", Methods Discourse)Post 108388 (missing)
(dormouse: "PdCl2 --> Pd(Ac)2. Help -sunlight", Novel Discourse)https://www.thevespiary.org/rhodium/Rhodium/chemistry/wacker.comments.txt (https://www.thevespiary.org/rhodium/Rhodium/chemistry/wacker.comments.txt)
Patent US3671590 (http://l2.espacenet.com/dips/viewer?PN=US3671590&CY=gb&LG=en&DB=EPD)
Patent US4638094 (http://l2.espacenet.com/dips/viewer?PN=US4638094&CY=gb&LG=en&DB=EPD)
Patent US3850990 (http://l2.espacenet.com/dips/viewer?PN=US3850990&CY=gb&LG=en&DB=EPD)
also tried both ethyl and methyl nitrate as oxidant.
You need to use an alkyl nitrite not nitrate.
But is a good dream. 100 cc of safrol single distilled ----->
81 grams of MDP2P.
It's my best one.
Post 107768 (missing)
BTW has Herr_Ovalmeister had success w/the patent he stated, or just believing what he reads?
I don't believe what you write.