The Vespiary

The Hive => Newbee Forum => Topic started by: pirat on April 18, 2003, 05:58:00 PM

Title: Is there any downside when i do not distill
Post by: pirat on April 18, 2003, 05:58:00 PM

buffered performic
bisulfite addition and recovering à la eleusis without distillation of the ketone!!
al/hg nitro
mdma
this really works

Is there any downside when i do not distill the ketone??

Title: bisulfite often yeilds gooey crystals that are
Post by: Antibody2 on April 18, 2003, 06:37:00 PM

bisulfite  often yeilds gooey crystals that are not really pure, these impurities carry over into subsequent rxns reducing yeild, causing side reactions and complicating further purification. but it can work to some extent

take the search engine out for a test drive there is plenty already posted on the subject