I feel like trying the protocol that LabTop wrote a long time ago on Rhodium's website. I will use the same ratios given by him.
I just have a question about it: He states to gas in chilled acetone. I was under the impression that gassing in acetone wasnt so good, as it can lead to a lot of side products. Am I right?
I will be doing a 1/10 of his write-up. How long should i let it stir in the end? I'm guessing, less then what's advised on his write-up since I'm doing 1/10 scale.
Any thoughts on this?