https://www.thevespiary.org/rhodium/Rhodium/chemistry/mdma.drdrool.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/mdma.drdrool.html)
. Then again I don't see how you could have gotten anything to come over at 100C with a simple distillation.Post 193368 (missing)
(OChem: "Nitromethane distillation probs", Newbee Forum)Post 107199 (missing)
(antibody: "Distilling nitromethane questions", Chemistry Discourse)Post 409914 (https://www.thevespiary.org/talk/index.php?topic=10931.msg40991400#msg40991400)
(experimentalbois: "60% Nitromethane", Newbee Forum)Post 358515 (https://www.thevespiary.org/talk/index.php?topic=9909.msg35851500#msg35851500)
(Bubbleplate: "Nitromethane Distillation Safety?", Methods Discourse)Post 285019 (missing)
(Rhodium: "Re: Nitromethane shelf life", General Discourse)https://www.thevespiary.org/rhodium/Rhodium/chemistry/equipment/pictures/distillation_big.jpg (https://www.thevespiary.org/rhodium/Rhodium/chemistry/equipment/pictures/distillation_big.jpg)
, warns against not using one.Post 269664 (missing)
(Chromic: "Re: 30% nitro methane", Chemicals & Equipment) and others seem to indicate that non-fractional distillation is okay. But keep in mind this will leave you with an azeotrope (mixture that cannot be seperated by simple distillation) of methanol/nitromethane.