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News / Re: Attorney accused of manufacturing hallucinogens!!!
« Last post by brb5min on December 08, 2023, 08:47:11 PM »I believe that synthed DMT has less smell than the extracted one. I would be quicker to smell residue of recrystallization solvent than the smell of synthed DMT.
xdragon, care to help a fellow newbie and share your workup with DMT oxalate? Do you use chloroform/DCM to extract from reaction mixture, and salt it out of this DCM? Or do I have to evap DCM first, crystallize from heptane and only then salt it out for rex? At which step should I attempt salting DMT out, I am not sure.
xdragon, care to help a fellow newbie and share your workup with DMT oxalate? Do you use chloroform/DCM to extract from reaction mixture, and salt it out of this DCM? Or do I have to evap DCM first, crystallize from heptane and only then salt it out for rex? At which step should I attempt salting DMT out, I am not sure.