How bout these ones?
Reaction Details 40 of 111
Reaction Classification Preparation
Yield 70 percent (BRN=105248)
Reagent potassium dichromate
Solvent dimethylformamide
Time 20 hour(s)
Other Conditions Ambient temperature
Ref. 1 5611749; Journal; Kim, Kwan Soo; Szarek, Walter A.; CRBRAT; Carbohydr.Res.; EN; 104; 1982; 328-333;
Ref. 1 5611749; Journal; Kim, Kwan Soo; Szarek, Walter A.; CRBRAT; Carbohydr.Res.; EN; 104; 1982; 328-333;
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Or this one...
Reaction Classification Preparation
Yield 92 percent (BRN=105248)
Reagent sodium bromite
Solvent H2O,acetic acid
Time 10 hour(s)
Other Conditions Ambient temperature
Ref. 1 5666548; Journal; Kageyama, Toshifumi; Kawahara, Shuji; Kitamura, Kohji; Ueno, Yoshio; Okawara, Makoto; CMLTAG;Chem.Lett.; EN; 1983; 1097-1100;
Q's, is sodium bromite made from sodium bromide? How? Huge temp, I bet?
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or this one...
Reaction Classification Preparation
Yield 95 percent (BRN=105248)
Reagent (bipy)H2CrOCl5
Solvent CH2Cl2
Time 4 hour(s)
Other Conditions Ambient temperature
Ref. 1 5574719; Journal; Chakraborty, T. K.; Bhushan, Vidya; Chandrasekaran, S.; IJSBDB; Indian J.Chem.Sect.B; EN; 22; 1;1983; 9-11;
Q's, what is H2CroC15?
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another...
Reaction Classification Preparation
Yield 95 percent (BRN=105248)
Reagent (1,10-phenanthroline)H2CrOCl5
Solvent CH2Cl2Time 8 hour(s)
Temperature 25 C
Ref. 1 5555229; Journal; Chakraborty, T. K.; Chandrasekaran, S.; TELEAY; Tetrahedron Lett.; EN; 21; 1980; 1583-1586;
Q's, reagent sounds a little obscure..
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or this...
Reaction Classification Preparation
Yield 80 percent Chromat (BRN=105248)
Catalyst CuO
Time 15 hour(s)
Temperature 200 C
Note 1 Further byproducts given
Ref. 1 5549295; Journal; Berthon, Bruno; Forestiere, Alain; Leleu, Gerard; Sillion, Bernard; TELEAY; Tetrahedron Lett.; FR; 22; 41; 1981; 4073-4076;
Looks too easy, heat at 200c with copper oxide for 15 hours and distill! Am I missing something?
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another....
Reaction Classification Preparation
Yield 86 percent (BRN=105248)
Reagent AcOOH/NaBr
Solvent ethyl acetate
Time 2 hour(s)Temperature 39.9 C
Ref. 1 5647691; Journal; Morimoto, Takashi; Hirano, Masao; Hamaguchi, Takayoshi; Shimoyama, Masahide; Zhuang, Xiumin; BCSJA8; Bull.Chem.Soc.Jpn.; EN; 65; 3; 1992; 703-706;
Sodium bromide and ethyl acetate is easy to get....
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Where can I go to look up these refs on the net?
Oh and Rhodium....you need to fix that page of references on your site coz there aint no 111 refs its about 80 with 40 of them repeated! You will see where Rev Drone signs out and then they are repeated from there.
One horny Bee!