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Author Topic: H20/Hcl extraction  (Read 2149 times)

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Vibrating_Lights

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H20/Hcl extraction
« on: February 15, 2002, 05:33:00 AM »
If one was expecting to have .5mole of mdma freebase in 2 L of toulene. then .5mole of hcl would be needed.  Sinceswim has 35%Hcl then aproximatly 50ml would be enough to extract all the amine,  correct?  How much water should be added to the 2 L of toulene prior to the titration?
VL_
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blaztoff

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Re: H20/Hcl extraction
« Reply #1 on: February 15, 2002, 06:17:00 AM »
Do several small extractions. One 100ml One 75ml One 50ml of a 5-10%Hcl solution. It dosnt take a lot of Hcl solution to dissolve youre freebase in. A little goes a long way.
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