quirks
Member posted 07-09-98 06:41 PM
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With small amounts like that you might of acidently added too much water to the rxn. 50% H2O2 is ~4/3 as heavy as water. 19.2 mls is ~25 grams. Opps!!
If the soloutions too orange gentle warming in water seems to push it over the hump and it'll gradually turn a deep red.
The other day someone who was not me was distilling precious md-p2p and there was only a little bit of tar left in the flask and it was starting to smoke but it was still coming over and god damn if he was going to stop before every last drop was over, anyways all of a sudden it went POOF and filled the top 1/3 of his condensor, the coloum and the flask with this fucked up plastic-black-glass stuff. Far, far more of it then the volume of tar that was in the flask. wtf is up with that???
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