?#1 when distilling my sassy is it 100% nessesary to have to add some buffer oil to it towards the end or just stop befor it burns in the flask and loose my last bit?
Forget distilling,freeze!!!Distilling you won't get it even nearly as pure as with freezing.Freezing is lot easier also.
?#2. one of my hot plate/stirrers has been modified to stay one all the time so it only stays on high heat. am i correct to assume it don't matter sence the oil wont get heated past its BP? or should i use anouter plate?
Use another plate,you need that to distill your ketone.
?#3. if doing say 250ml of sassy is an oil bath 100% nessisary or can a fbf be used instead. as long as it don't implode from the vac. i took my whole rig down to 15 torr. with noting in it to see if it could handle the vac and it din't implode on me.
See question 1
when doing the methanol wacker. witch alc is the best to use? i have acsess to ethanol,anhydrous methanol. and anhydrous isp.alc. wich is best and why?
Doesn't really matter,but use methanol,it's easier to get rid of it later as has lowest bp of em all.
when i am done wacking my oil in the wacker. can i just vac filter it a few times. then throw it in a flask and fractinaly distill off the alc. then collect my fraction containing my p2p?
Probably yes,but i'm not familiar with this rx so i can't tell for sure.
?#6 when doing the Nitromethane Al/Hg reduction will an indented 2,000 ml flask be ok to use? thats all i have.
Depends how large rx you are planning to dream
?$7 what condenser should i use? i have a 4 bulb allin seems the easiest to clean after. but dont seem like it will be big enought to contain every thing if it gets out of hand. i have a 500mm liebig also. and a fredric but the freddi seems like it would be a bitch to clean should any thing puke up in to it. shit what to use what to use?? should i just go ineny meany miney mo? or rock paper scissors?
See previous question.Your condenser won't get filled with shit.
?#8 how smelly is the Nitromethane Al/Hg resuction? if my condenser is good enought will it stink up the lab? will a ballon over the end of the condenser be ok or not ok to do?
Doesn't really depend which condenser you use,methyamine bp is below zero C so it'll get out anyway.Depends how hot is you rx mix.
?#9 i have a few gallons of nice distilled pet ether. can that be used for my NP when extracting my goods? also could distilled turpentine or turpinoid be used at all?
Pet ether will probably work.
?#10 do i HAVE to gas my finel product? can i just titrate it from my NP in to DH20 and evap my water? the only reason i don't want to gas is i dont have any H2SO4 right now. inless i take it out of an old car battery i have out in the barn. would lead in the battery cause any problums? could i do it using foil and hydrochloric as long as i dry the cock out if it?
and one last one that should of been closer to the top. when doing my Al/Hg would it be ok to add a few mg more HgCl2. and if not whats the reason not to.
Battery acid doesn't work,you could also titrate freebase in acetone and it'll will precipate if you 3-base was pure,if otherwise,you won't probably see any nice crystals at all and may just titrate in water and evapp.Rxtal would be nice.You may add as much HgCl2 as you want but emptying 100 gram HgCl2 bottle to amalgamate 25 grams of foil is not right thing to do,however,cuz it costs pretty much.