Author Topic: problem with performic yields  (Read 5970 times)

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abacus

  • Guest
Don't get too sidetracked.
« Reply #20 on: December 10, 2002, 11:15:00 AM »
Ketone can easily be distilled at reduced pressure up to 200DegC with no loss of yield IME so don't get too worried about losing yield at the temperatures you distill at.

74% molar yield from buffered performic (including hydrolysis refluxing for 3 hours) is exactly as expected.

Abacus

carcrash

  • Guest
yeah dielectic silicon grease
« Reply #21 on: December 14, 2002, 10:48:00 AM »
Spark plug grease. 

Not a chemist I just follow directions on the box mix